Publication Type Journal Article
Title Diethyl 4,4 -(ethane-1,2-diyldioxy)dibenzoate
Authors Zhen Ma Huang Yang
Groups
Journal ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE
Year 2011
Month July
Volume 67
Number 7
Pages O1623-U124
Abstract The title compound, C20H22O6, was obtained by the reaction of ethyl 4-hydroxybenzoate with 1,2-dichloroethane in dimethylformamide. The molecule lies around the crystallographic inversion center at (0,0,0), with the asymmetric unit consisting of one half of the molecule. The two ethyl groups are in trans positions. The ethyl, carboxyl, aryl and O-CH2 groups are coplanar with an r.m.s. deviation of 0.0208 (9) angstrom. The whole molecule is planar with an r.m.s. deviation of 0.0238 (9) angstrom for the 19 atoms used in the calculation and 0.0071 (9) angstrom for the two aryl groups in the molecule. A weak intermolecular C-H center dot center dot center dot O hydrogen bond and a C-H center dot center dot center dot pi interaction help to consolidate the three-dimensional network.
DOI http://dx.doi.org/10.1107/S1600536811021258
ISBN
Publisher
Book Title
ISSN 1600-5368
EISSN
Conference Name
Bibtex ID ISI:000294663200001
Observations
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